Synthesis of 32P-Labelled Dimethylamido Ethoxyphosphoryl Cyanide (Tabun).
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چکیده
منابع مشابه
Synthesis of [32P]dolichyl phosphate, utilizing a general procedure for [32P]phosphorus oxychloride preparation.
Equilibration of the phosphorus in radioactive phosphoric acid with the phosphorus in phosphorus oxychloride occurs if these compounds are refluxed together for approximately 24 h. This observation led us to develop a method for the preparation of radioactive phosphorus oxychloride on a small scale with high specific radioactivity. The labeled phosphorus oxychloride may be utilized directly in ...
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In previous papers (McMurray, Strickland, Berry & Rossiter, 1957b; McMurray, Berry & Rossiter, 1957a) two systems capable of supporting the incorporation of inorganic 32p into the phospholipids of rat-brain dispersions were described: (a) an anaerobic system (best demonstrated in hypotonic dispersions), which supported the labelling of lipid P under optimum conditions for glycolysis (McMurray e...
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Discovery of 13C NMR and its application in the biosynthetic pathways prompted the synthesis of several 13C labelled precursors. To investigate the metabolism of phenyllactic acid in the Solanaceae family, the double labelled acid was synthesized from barium carbonate (13C) and sodium syanide (13C)
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"Soluble" (KFe(III)[Fe(II)(CN)6]) and "insoluble Prussian blue" (Fe(III)4[Fe(II)(CN)6]3 labelled with 59Fe either in the ferric (Fe(III)) or ferro (Fe(II)) position and 14C in the cyanide group were synthesized and administered intraperitoneally or orally to adult female rats with normal body iron stores. Following i.p. injection of KFe[Fe(CN)6], the colloidal complex is disintegrated into ferr...
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A simple and rapid assay method is described for determining the specific radioactivity of the gamma-phosphate group of 32P-labelled ATP. Labelled ATP is incubated with cyclic AMP, cyclic AMP-dependent protein kinase and histone H2A under conditions leading to maximum phosphorylation of the histone. The specific radioactivity of the gamma-phosphate group of the 32P-labelled ATP is calculated fr...
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ژورنال
عنوان ژورنال: Acta Chemica Scandinavica
سال: 1963
ISSN: 0904-213X
DOI: 10.3891/acta.chem.scand.17-2688